Synthesis and Characterization of Porphyrin Based Macromolecule and its Metal Complex

Authors

  • Dr. Naimish K Chavda  M.G.Science Institute Ahmedabad, Gujarat, India

Keywords:

Porphyrin; Spectral analyses; Metal complex;

Abstract

The new porphyrin based ligands has been synthesized and characterized using FAB-mass spectroscopy,1HNMR,13CNMR and UV-Vis spectrophotometry. The NMR confirmed the structure of the compound and the mass spectrum was in agreement with the proposed molecular formula. The UV-Vis absorption spectrum of synthesized compound shows characteristic spectral patterns similar to proposed structure with a Soret band at 419 nm and four Q bands at 515, 550, 590, and 648 nm. Protonation of the porphyrin with TFA resulted in the expected red shift of the Soret band. Excitation at 419nm gave an emission at 650nm. Metal complex of the newly synthesized porphyrin ligand was synthesized and characterized by various analytical techniques.

International Journal of Scientific Research in Chemistry

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Published

2018-02-26

Issue

Volume 3, Issue 3, January-February-2018

Section

Research Articles

License

Copyright (c) IJSRCH

Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.

How to Cite

[1]
Dr. Naimish K Chavda, " Synthesis and Characterization of Porphyrin Based Macromolecule and its Metal Complex, International Journal of Scientific Research in Chemistry(IJSRCH), ISSN : 2456-8457, Volume 3, Issue 3, pp.37, January-February-2018.